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O hydrogen bonds link the mononuclear units into a three-dimensional
network. The morpholine unit adopts an almost ideal chair conformation.
S interactions about an inversion center.
N hydrogen bonds are observed in the crystal structure. The CoII ion is
six-coordinated by four O atoms of methanol molecules and two water
molecules in a distorted octahedral geometry. In the dianion, one of the
sulfate groups is unidentate whereas the other two chelate the metal
atom.
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S interactions about an inversion center.
The MnII atom is coordinated by four N atoms of two phen ligands, one Cl
atom and one aqua ligand, forming a distorted octahedral geometry.
O hydrogen bonds stabilize the crystal packing. The piperidine ring
adopts a chair conformation in both molecules. The morpholine unit
adopts an almost ideal chair conformation. Cl interactions, along with
S. O hydrogen bonds link the molecules, forming infinite chains. In each
molecule, the Mn atoms have octahedral geometry with two coordinated
pyridines bonded to two MnIII and a terminal pivalic acid coordinated to
the MnII atom. The axial positions are occupied by N atoms of two
monodentate dicyanamide anions. The complex molecules are connected
through intermolecular hydrogen bonds, forming a two-dimensional layer
structure.
The square pyramid is completed by an aqua ligand in the apical
position. The Cu atom is located on a twofold axis.
A three-dimensional supramolecular network is formed by intermolecular
hydrogen bonds.
The complex molecules are connected through intermolecular hydrogen
bonds, forming a two-dimensional layer structure. The two imino ligands
are mutually trans. In the crystal strucure, cations and anions are
linked into a three-dimensional network architecture by hydrogen bonds.
Both the cation and anion lie about mirror planes.
The square pyramid is completed by an aqua ligand in the apical
position. O hydrogen bonds that link adjacent molecules into
one-dimensional chains.
O hydrogen bonds, generating a three-dimensional network. The MnII atom
is coordinated by four N atoms of two phen ligands, one Cl atom and one
aqua ligand, forming a distorted octahedral geometry. In the dianion,
one of the sulfate groups is unidentate whereas the other two chelate
the metal atom. In the dianion, one of the sulfate groups is unidentate
whereas the other two chelate the metal atom.
A three-dimensional supramolecular network is formed by intermolecular
hydrogen bonds. A three-dimensional supramolecular network is formed by
intermolecular hydrogen bonds. N hydrogen bonding between the imine H
atom and the oxime N atom. The six-membered ring consisting of the two
Pd atoms and the four pyrazole N atoms has a boat-shaped conformation.
In the crystal structure, each naphthaleneacetate ligand coordinates two
metal centres through its carboxylate O atoms, adopting a
bis-monodentate mode to give rise to a two-dimensional network. The
CoIII centre has a distorted octahedral geometry in both molecules. Cl
interactions, along with S.
The cations form separate, enantiomerically pure columns along the
a-axis direction.
N hydrogen bonding between the imine H atom and the oxime N atom. S
interactions about an inversion center. O hydrogen bonds, which link the
molecules into chains running parallel to the c axis. S interactions
about an inversion center.
The six atoms around the metal form a slightly distorted octahedral
geometry.
Acylhydrazines are an important synthon used to construct hydrogen-bond
networks.
The central Bi atom is eight-coordinate in a capped distorted pentagonal
bipyramidal geometry.
O hydrogen bonds that link adjacent molecules into one-dimensional
chains.
One of the four ethyl groups of the cation is disordered.
The piperidine ring adopts a chair conformation in both molecules. O
hydrogen bonds that link adjacent molecules into one-dimensional chains.
Acylhydrazines are an important synthon used to construct hydrogen-bond
networks. Cl intermolecular hydrogen bonding. The central Bi atom is
eight-coordinate in a capped distorted pentagonal bipyramidal geometry.
The complex molecules are connected through intermolecular hydrogen
bonds, forming a two-dimensional layer structure.
The axial positions are occupied by N atoms of two monodentate
dicyanamide anions. The two imino ligands are mutually trans. Cl
hydrogen bonds stabilize the crystal structure.
The morpholine unit adopts an almost ideal chair conformation.
N hydrogen bonding between the imine H atom and the oxime N atom. S
hydrogen bonds link the molecules into centrosymmetric dimers.
O hydrogen bonds, which link the molecules into chains running parallel
to the c axis.
S hydrogen bonds link the molecules into centrosymmetric dimers.
Acylhydrazines are an important synthon used to construct hydrogen-bond
networks. The crystal structure contains sheets perpendicular to the bc
plane. The cations form separate, enantiomerically pure columns along
the a-axis direction.
The Ni atoms both show a square-planar coordination geometry.
N hydrogen bonding between the imine H atom and the oxime N atom.
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